Open Access Repository

Differential ion mobility spectrometry with temperature programmable micromachined gas chromatography for the determination of bis(chloromethyl) ether

Luong, J, Gras, R and Shellie, RA ORCID: 0000-0002-8470-0893 2017 , 'Differential ion mobility spectrometry with temperature programmable micromachined gas chromatography for the determination of bis(chloromethyl) ether' , Analytical Methods, vol. 9, no. 34 , pp. 5003-5008 , doi: 10.1039/c7ay00653e.

Full text not available from this repository.

Abstract

A parts-per-million level screening technique for bis(chloromethyl)ether using micromachined differential ion mobility spectrometry combined with portable temperature programmable low thermal mass silicon micromachined gas chromatography is described. With its capability to operate in atmospheric pressure, the analytical system affords fast start-up with a high sample throughput. The technique described can be used to screen for bis(chloromethyl)ether in ambient air directly without pre-concentration or derivatization with a low possibility of false positive results. A complete analysis can be carried out in less than 240 s. A detection limit of 2 μL L−1 and relative precision of less than 5% RSD (n = 10) over a range from 5 μL L−1 to 500 μL L−1 were obtained.

Item Type: Article
Authors/Creators:Luong, J and Gras, R and Shellie, RA
Keywords: spectrometry, gas chromatography, bis(chloromethyl)ether detection
Journal or Publication Title: Analytical Methods
Publisher: Royal Society of Chemistry
ISSN: 1759-9660
DOI / ID Number: 10.1039/c7ay00653e
Copyright Information:

Copyright 2017 The Royal Society of Chemistry

Related URLs:
Item Statistics: View statistics for this item

Actions (login required)

Item Control Page Item Control Page
TOP