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Capstone laboratory experiment investigating key features of palladium-catalyzed Suzuki−Miyaura cross-coupling reactions

Pullen, R, Olding, A, SMith, JA ORCID: 0000-0001-6313-3298 and Bissember, AC ORCID: 0000-0001-5515-2878 2018 , 'Capstone laboratory experiment investigating key features of palladium-catalyzed Suzuki−Miyaura cross-coupling reactions' , Journal of Chemical Education , pp. 1-5 , doi: 10.1021/acs.jchemed.7b00964.

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Abstract

This two-part laboratory experiment is concerned with investigating key aspects of the Suzuki-Miyaura cross-coupling reaction. The first part of this experiment utilizes high-throughput experimentation techniques to reinforce, explore, and extend fundamental concepts that are presented in the classroom. In contrast, the second part employs guided-inquiry learning strategies to challenge students to design, set up, and perform a preparative-scale Suzuki-Miyaura reaction and suggest workup and isolation protocols. By design, this experiment, which represents one of the final experiments performed in the third-year undergraduate chemistry laboratory program, serves as a capstone learning experience for students.

Item Type: Article
Authors/Creators:Pullen, R and Olding, A and SMith, JA and Bissember, AC
Keywords: laboratory instruction. inquiry-based/discovery learning, catalysis
Journal or Publication Title: Journal of Chemical Education
Publisher: Amer Chemical Soc
ISSN: 0021-9584
DOI / ID Number: 10.1021/acs.jchemed.7b00964
Copyright Information:

Copyright 2018 American Chemical Society and Division of Chemical Education, Inc.

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